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Affordable nano powder handling

Written by Robert Greenyer on .

It is exciting times here because in the next 10 days we expect to receive 75um powder from Dr. Brian Ahern and 10nm Ni from Quantum Sphere to join the special powders Bob Higgins has produced, which are also in the micro-metric range.

Brian's 10nm Ni/Pd islands in ZrO grains will need significant further processing to get them down to around 15um and this will take some weeks of grinding and we are still discussing how best to do that as the raw material is very precious.

Bob Higgins' and Brian's powders are big enough, even after grinding to operating sizes, to not loft easily (do not become airborne) and they also do not present the same health hazard that the 10nm QSI Ni may present, from inhalation, skin and eye exposure. That is not the only challenge Ni at this size presents as Ryan found out when handling their 40nm Ni powders... with even just a little humidity, these particles start to clump together and then become difficult to handle and potentially inactive. So we need to find a way to safely handle these materials whilst keeping them dry, some of the early options we were considering looked really expensive, but Alan Goldwater has been doing some great work trying to make this part of the process affordable.

First was the getting the cost of the "glove box" down... In Alan's words "Barring some serious DIY, a dry glove box looks to be expensive, even used. The basic CLEATECH plastic ones are $1k+ on eBay, and the metal ones more." That is not really practical for wide scale testing, so he looked for other options and found that a glove bag purged with Argon or Nitrogen could work with a variety of sizes available for $20-30...

Glove bag supplier 

Alan adds "The nice thing about a glove bag is that after loading it, you can collapse and squeeze it to get the air out, then inflate it with dry gas. Seems to me 2 cycles of that should get down to less than 10% relative humidity (RH). So figure 4 cubic feet of gas per use (for the smallest size bag from the above source). Another advantage is that when you're done with the job, just crumple the bag up and toss it, so nano-contamination of the enclosure is not an ongoing issue. Still have to wash the scale, implements and bottles..."

Suitability test

Alan sought to test the potential of the glove bag concept, combined with a desiccant, to get to below the 10% (RH) target. 

  1. On the advice of Mathieu, he bought a WH8040 Digital Air Humidity Controller Sensor for $30.39 from Amazon.com which has a measuring range from 1%-99% AC 110V. It's also available for 220 v.a.c. supply on Amazon.co.uk, about £20.
  2. He then activated an 8 oz silica gel fabric bag he had, by baking it at 120 C for 150 minutes, followed by 30 minutes in a convection oven (a fruit dryer) at 50 C to remove residual water vapour.
  3. He then used a polythene bag, about 2 mil thick and 10 litre volume. He filled it with ambient air at 48% RH and then added the activated silica gel cotton bag, the RH sensor probe and closed up the bag with a wire-tie. 

Figure 1: Test setup

Results

In Alan's words "After 15 minutes the meter read 20%, and at 30 minutes it was 3.5%...

...At 45 minutes, it's "off the scale" - less than 1% with this meter. Accuracy is probably ±5% at best and no calibration was attempted. But even if its ±10%, the desiccant seems to do the job."

Conclusion

Using a $30 glove bag and some activated silica gel looks like it will really work! Additionally, if the powder did not have a problem with dry air, then there would be no need for Argon or nitrogen. A Big thank you goes to Alan for taking the initiative on this one. By testing the humidity meter with an actual glove bag and more silica gel, we could develop a protocol for Nano Powder handling that would not require the RH meter so cutting the cost of this part of the process to essentially that of the glove bag.

Discussion

We are expecting to receive 4 packages of 5g of 10nm QSI powder and this will be required to be handled in 3 locations, Minnesota (testing in advanced powder reactor), France (testing in high pressure Mizuno style cell) and California (partial sintering on Ni mesh substrate for later glow discharge testing). So this finding, especially proper use of silica gel, will be immediately helpful.

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I didn’t know roof repairs could be done so quickly. This article has motivated me to schedule an appointment.
Thanks for the helpfull information!
Has anyone else faced the dillemma of roof repairs
versus replacement? This post made me realize how important it iss tto consult a roofing
expert before makinhg a decision.
Turns out there’s a llot moe to it, like assessing overall condition and addressing underrlying issues.
I’ll be booking ann inspection to figure out what I need.

Thanks for the clarity!
I’ve been delaying roof repairs because I wasn’tsure if it was really necessary.

I’ll definitely be getting my roof checked soon.
Great advice here!
I’ve been on the fence about whether to replace or repair my roof.
The ttips here helped me understand how to make a more informed decision. Thanjs for sharing this valuable info.

I had no idea that roof age pplayed such a big rlle in determining whether to repair or replace.
I’ll keep that in mind as I move forward with
my roof issues.
I had a roof replacement done last year, and I can’t stress enough how much better iit feels.
If anyone is hesitant about replacing their
roof, I highly recommend considering it. It really makes a difference.


Whaat a helpful post! I’ll definitely follow your advice aand have my roof inspected efore makking aany decisions.

I’ve been trying to delay repairs, but it’s becoming clear I need to address tthe issues
sooner rather than later. I’ll be contacting a professional soon.
I’ve been thinking about getting a new rlof for a while, bbut wasn’t sure
if it was worth the cost. Thanks for the helpful information—I think it’s time
for an upgrade.
My roof is showing signs of age, and now I realize how important itt
is to take care of it. I’ll definitely follow upp with a roof inspection to see what’s needed.

I’ve had some roofing issues for a while but wasn’t sure whether to
replace or just repair. This blog has really opened my eyes to the importance oof getting a
professional inspection. I think I’ll reach out to
get some expert advice.
I always thought a roof replacement would be a huge hassle.
I’ll definitely keep this in mind when it’s time to replace mine.
Thanks for the helpful breakdown!
I’ve been putting off roof repairs, but now I understand
that addressing small iswues early can save a lot in the future.

I’ll be contacting a roofing professional to taie a lok
att my roof.
I’m going to make sure I get my roof inspected soon to avoid anyy bigger problems.
This post really helped me understand why
regular roof maintenance is so important.

I recently had a major leak, and this post helped me figure out whether
I should repaijr or replace my roof. I’ll be following up with a professional soon.
I’ve been putting it off, but now I see it could save
mme a lot of trouble in the future. Thanks for the insightful information!
Great post! It’s good to know that a new roof can not only prevent leaks but also boost my home’s value.
I’m definitely considering my options now.

Here is my web site - Roof maintenance tips.: Butlerroofingaberdeen.carrd.co /
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